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The Desulfurization & Denitrification of Coker Gasoline by Heteropoly Acid
LI Yun,WANG Xiang-fu,GUO Da-guang, JI Cheng-cheng,YAN Feng,XU Yao-hui
Abstract
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386
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271
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The oxidation desulfurization and denitrification of coker gasoline were carried out with hydrogen peroxide as the oxidant, phosphorus tungsten acid as catalyst, cetyl trimethyl ammonium chloride as phase transfer catalysts and furfural as extracting agent. The desulfurization and denitrification rate can reach to 89.93% and 95.10% under the following conditions: gasoline 50 mL, catalyst 0.32 g, phase transfer catalyst 0.09 g, hydrogen peroxide 5 mL, oxidation temperature 70 ℃, oxidation time 60 min. The Oxidant Solution can be recycled when replenishing appropriate oxidant and phase transfer catalysts, and the extractant can also be recycled after treatment. Without phase transfer catalyst, the desulphurization and denitrification rate were only 77.35% and 91.98%, respectively. Therefore, phase transfer catalyst can greatly improve the desulfurization performance.
2012, 32 (4): 4-7.
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Process Optimization for Refining Used Industrial Lubricating Oil by Solvent Method
WU Tong,GUO Da-guang,LIU Yang
Abstract
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421
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305
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Two methods including furfural refining and dual-solvent (2-Propanol and furfural) refining were investigated respectively in recycling the used industrial lubricating oil. The results show that the performance of dual-solvent refining is better than furfural refining. The optimum process condition is as follows: refining temperature 75 ℃, volume ratio of solvent 2-Propanol to furfural 1∶1, volume ratio of solvent to oil ratio 1.5∶1. Under these optimum conditions, the physical properties[KG*2]of[KG*2]recycled[KG*2]oil is[KG*2]listed[KG*2]as[KG*2]follows:[KG*2]viscosity[KG*2]index[KG*2]119.5,[KG*2]refractive[KG*3]index[KG*3]1.476[KG*3]6,[KG*3]Color[KG*3]1.0,[KG*3]freezing[KG*3]point -15.8 ℃, flash point 218.4 ℃ , sulfur content 0.026%, the total oil yield 72.5%.
2012, 32 (2): 16-19.
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Recovery of Vehicle Waste Lubricant Oil by Cosolvent Refined Method
LIU Yang, GUO Da-guang*, WU Tong, LI Shi-song
Abstract
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348
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The refining of vehicle waste lubricant oil using the furfural as the main solvent and sodium dodecyl benzene sulfonate as the cosolvent were studied. The influence of mixed solvent ratio, extraction temperature and other factors on the yield and quality of recovery refined oil are also investigated. It turns out that when the temperature is 80 ℃, the catalyst oil ratio is 1.5, the additive precentage of sodium dodecyl benzene sulfonate is 0.025%, the properties of refined oil with high yield[KG*3](91.26%)[KG*3]is[KG*3]listed[KG*3]as follows: the viscosity index is 116.83, the refractometer index on 25 ℃ is 1.441, the chromatic is 2.0, the condensation point -19 ℃, w(carbon residue) is 0.496%. The refined lubricated oil after adding some additive can meet the requirements of lubricant oil, and can be reused.
2011, 31 (4): 5-08.
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Recycling Process of Industrial Waste Lubricating Oil
HAN Li-jun, REN Ya-lin, WU Tong, GUO Da-guang
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482
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216
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The refining of industrial waste lubricating oil was investigated with N-methyl-2-pyrrolidone (NMP) and Duo-solvent (ethanolamine and NMP) as solvents, respectively. The preferred refining process is duo-solvent refining under 70 ℃ with 5% ethanolamine, under these conditions the total oil yield was 89.85%. The physical properties of recycled oil is listed as follows: viscosity(40 ℃) 30.89 mm
2
•s
-1
, viscosity(100 ℃) 5.6 mm
2
•s
-1
, viscosity index 120.4, refractive index 1.450, Color 2.0, freezing point -28.8 ℃, flash point 219.6 ℃ and sulfur content 0.057%.
2010, 30 (4): 11-14.
DOI:
10.3696/j.issn.1672-6952.2010.04.004
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Recycle the Used Lubricating Oil by Di-Solvent Refining
LI Lu, GUO Da-guang*, WU Tong
Abstract
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381
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250
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Di-solvent is composed with epichlorohydrin and furfural. Two methods of furfural and di-solvent were investigated in recycle the used lubricating oil for effects. The experimental results show that the optimal technology conditions of di-solvent refining are the volume ratio of oxidant to oil 1.0 and V(epichlorohydrin)∶V(furfural) 1.5∶1. The optimal technology condition of furfural refining is the volume ratio of oxidant to oil 1.5 .Under the optimal technology conditions, the used engine oil total yield reach 73.95%. The properties of the recovered oil are viscosity index at 118.4, after append to a process of clay-adsorption, the recovered oil could be circularly used by harmonicing of proper quantities additions.
2009, 29 (4): 30-33.
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Technology of Recovering Used Lubricating Oil
LI Lu, GUO Da-guang, MO Ya-nan
Abstract
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416
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378
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The flocculation refining and solvent refining experiments was carried out to show that solvent refining is better for the recycling the lubricating oil waste. The optimal conditions of furfural refining were as follows: the ratio of solvent and oil 1.5, refining temperature 80 ℃|while the optimal condition of NMP refining was 1.0, refining temperature 60 ℃, so the furfural refining had a larger economic profits. Under the optimal technology conditions, the properties of the recovered oil were listed as follows: viscosity index 102.6, 25 ℃ refractive index 1.459 4, colourity 1.0, solidifying point -16 ℃, w(carbon residual)0.499%, w(S)0.057%, oil recovery 93.96%. According to this result, the recovered oil could reach the HVI standard of base oil. And the recovered oil could be used as finished lubricating oil after adding suitable amounts of additives.
2008, 28 (4): 20-23.